Advanced technology high performance tank linings are often applied by plural spray equipment and occasionally one of the components could be off-ratio. Worse still, some well-intentioned field personnel might add more curing agent to speed up the cure, or alter other properties, or may not utilize the entire curing agent portion in a single leg application.

This paper investigates the effects of under-cure or over-cure on the performance of two high temperature tank linings by deliberately mis-mixing the two components.

Accelerated laboratory tests were undertaken on a 2ct thin film solvented polycyclamine cured epoxy and a 1ct solvent-free, thick film polycyclamine cured epoxy. The tests employed were autoclave (TM0185) at high temperature in oilpatch production fluids, electrochemical impedance spectroscopy (EIS), adhesion, solvent resistance, infra-red spectroscopy, differential scanning calorimetry (DSC), and dry time observations.

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